50 min

S1 E08 - Devolatilization & Cannabinoid Distillation The Modern Extractor

    • Chemistry

Look no further for DISTILLATION SOPs!
Jay Horton joins us to discuss getting maximum throughput and high quality distillates out of you wiped film distillation unit. We cover specific SOPs for terpenoid removal (terp strip) and cannabinoid distillation for both THC and CBD. We discuss getting maximum throughput on a single stage machine, as well as various ways to configure your multi stage distillation unit to maximize your results. Jay's 'split the stream' technique will get you the highest quality and largest quantity yields out of your multi-stage wiper.
EPISODE TRANSCRIPT:
Jason Showard - 00:00:11 
Hello and welcome to Episode eight of The Modern Extractor. This podcast focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through lab, as material makes its way from Cultivar to concentrate. 
 
Jason Showard - 00:00:37 
Last week we had John Hart, founder and CEO of Chemtech Services, on the show to talk about wiped film and rolled film distillation. He broke down what's going on inside of a wiped film distillation unit and helped make some sense of it. He hit us with a ton of distillation knowledge gained through his years of experience building high tech equipment for the chemical industry. Moving on to this week's show, let's catch back up with our work in progress. So far, we've performed a cold ethanol extraction in the centrifuge. 
 
Jason Showard - 00:01:03 
We've cold filtered the resulting miscella through a lenticular filter. We ran the filtered miscella through a falling film evaporator to separate the oil and the ethanol. And we decarboxylated the crude oil, converting the THC A or CBD A into THC or CBD. This week we're going to get into specific SOPs for removal of the terpenoids, also known as terp stripping, followed by distillation of THC and CBD. It's a big day today guys. We're finally going to make some sellable product. 
 
Jason Showard - 00:01:30 
Joining me on the show today is the man that got me started distilling cannabinoids. He's usually flying around the world installing and training on Chemtech's distillation equipment, or doing some type of cannabis lab consulting. He's the founder of Genovations and quite a veteran in the cannabis lab space. Jay Horton, welcome to The Modern Extractor. 
 
Jay Horton - 00:01:47 
Hello, Jason. 
 
Jason Showard - 00:01:48 
Where are you calling in from today? 
 
Jay Horton - 00:01:49 
I'm currently in Los Angeles. 
 
Jason Showard - 00:01:51 
All right. Yeah, I'm also here in Los Angeles, still hunkering down. So I met you years ago when you installed the first wiped film unit I ever worked with, at the company I was working for. It was a Chemtech Mini 5. By the time we were done, strapping upgrades to it, it was almost KD6. Since then, you started your own company, Genovations. Tell us a little bit about how you got into the field and what the path was like to starting your own business. 
 
Jay Horton - 00:02:20 
OK, so in around 2006, I moved to Oregon and got into the medical program and I was doing cultivation. In around 2013, I started working with the company that was looking into CO2 extraction very early on. We

Look no further for DISTILLATION SOPs!
Jay Horton joins us to discuss getting maximum throughput and high quality distillates out of you wiped film distillation unit. We cover specific SOPs for terpenoid removal (terp strip) and cannabinoid distillation for both THC and CBD. We discuss getting maximum throughput on a single stage machine, as well as various ways to configure your multi stage distillation unit to maximize your results. Jay's 'split the stream' technique will get you the highest quality and largest quantity yields out of your multi-stage wiper.
EPISODE TRANSCRIPT:
Jason Showard - 00:00:11 
Hello and welcome to Episode eight of The Modern Extractor. This podcast focuses on the processes, equipment and science found in a cannabis extraction laboratory. I'm your host Jason Showard, and I work professionally in the cannabis extraction field. Here in season one, we're focusing on ethanol extraction and post processing. With each episode digging deep into a particular stage in that process. The shows are released in an order that follows the workflow through lab, as material makes its way from Cultivar to concentrate. 
 
Jason Showard - 00:00:37 
Last week we had John Hart, founder and CEO of Chemtech Services, on the show to talk about wiped film and rolled film distillation. He broke down what's going on inside of a wiped film distillation unit and helped make some sense of it. He hit us with a ton of distillation knowledge gained through his years of experience building high tech equipment for the chemical industry. Moving on to this week's show, let's catch back up with our work in progress. So far, we've performed a cold ethanol extraction in the centrifuge. 
 
Jason Showard - 00:01:03 
We've cold filtered the resulting miscella through a lenticular filter. We ran the filtered miscella through a falling film evaporator to separate the oil and the ethanol. And we decarboxylated the crude oil, converting the THC A or CBD A into THC or CBD. This week we're going to get into specific SOPs for removal of the terpenoids, also known as terp stripping, followed by distillation of THC and CBD. It's a big day today guys. We're finally going to make some sellable product. 
 
Jason Showard - 00:01:30 
Joining me on the show today is the man that got me started distilling cannabinoids. He's usually flying around the world installing and training on Chemtech's distillation equipment, or doing some type of cannabis lab consulting. He's the founder of Genovations and quite a veteran in the cannabis lab space. Jay Horton, welcome to The Modern Extractor. 
 
Jay Horton - 00:01:47 
Hello, Jason. 
 
Jason Showard - 00:01:48 
Where are you calling in from today? 
 
Jay Horton - 00:01:49 
I'm currently in Los Angeles. 
 
Jason Showard - 00:01:51 
All right. Yeah, I'm also here in Los Angeles, still hunkering down. So I met you years ago when you installed the first wiped film unit I ever worked with, at the company I was working for. It was a Chemtech Mini 5. By the time we were done, strapping upgrades to it, it was almost KD6. Since then, you started your own company, Genovations. Tell us a little bit about how you got into the field and what the path was like to starting your own business. 
 
Jay Horton - 00:02:20 
OK, so in around 2006, I moved to Oregon and got into the medical program and I was doing cultivation. In around 2013, I started working with the company that was looking into CO2 extraction very early on. We

50 min